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GC/MS analysis results for sample AD23084, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23084 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087904–000087919

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C : \HPCHEM\ 1 \DATA\OCT04 01 \'2 3 0 84 . D Vial: 4 Acq On ‘ 4 Oct 2001 6:27 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise .Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Hexatriacontane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

32.75 0.42 ug/1 67068 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane ' 507 C36H74 000630-06-8 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Pentacosane 352 C25H52 _____ 000629-99-2 91 SSbundance Scan 3019 (32.754 min): 23084.D (-) m/z 57.00’ 100.00% 7 71 43 85 5000 Ti* .-T-?-? f-. r, I 1 , "rn *rr (■ ? 99 113 127 141 155 169 32.40 32.60 32.80 33.00 m/z 71.00 74.39% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #74636: Hexatriacontane 43 5(7

I 71 ! 5000- t i1 85 32.40 32.60 32.80 33.00 97 m/z 43.05 64.02% J ] !.l 127 141 155 169 183 197 211 m/z-> 40 60 80 100 120 140 160 180 200 22o' 240 260 280 300 Abundance #42201; Heneicosane 57 71 , fYfTS''f9"! : 85 32.40 32.60 32.80 33.00 5000 m/z 85.05 50.81% 99 , 127 141 155 K 268 296 m/z--> 40 ' ' 60 80 ioO 120 140 160 180 200 220 240 260 280 300 Abundance #32063: Heptadecane Ma ’ ‘ I ' 7 32.40 32.60 32.80 33.00 71 m/z 41.05 25.78% 85 5000 99 I 196 240 J ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 32.40 32.60 32.80 33.00

23084.D NP091101.M Tue Oct 09 12:29:35 2001 Page 5

NYC-WTC_000087915

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NYC-WTC_000087915Source: NYC Law Department, mirrored locally

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