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GC/MS analysis report for sample AD22544, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22544 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086913–000086932

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000086926
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22544.D Vial: 10 Acq On : 25 Sep 2001 11:15 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Docosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 32.76 0.45 ug/1 56768 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Docosane 310 C22H46 000629-97-0 9h 2 Heneicosane 296 C21H44 000629-94-7 91 3 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91 4 Tetratetracontane 619 C44H90 007098-22-8 91^ Abundance Scan 3020 (32.762 min): 22544.D (-) m/z 57.00 100.00%! 7

85 5000 4' 3Z40 3Z60 3280 3ig0

Ti/z-> ... ________??___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 m/z71.10 66.57% ^bundance #44318: Docosane 7

85 I . I , I i-pi ., / I k I I I , I I 550 32.40 32.60 32.80 33.00 m/z 43.00 63.99% 266 310 -rrp Yrrrry-rTTry^rT-rTYrri-ryrTTrYrri-rYrrrTYrTTT-^^^ I "I pVr-r I ‘ ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #42201; Heneicosane 5|7

85 32.40 32.60 32.80 33,00 550 m/z 85.05 51.12%

I 113 268 296 I' "'I" '' I" '' I p-n-rp-n-tp I ” '' r ‘ " I Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance 57 #49558: Heptadecane, 9-octyl- A -Y-Tp-T 32.40 32.60 32.80 33.00 m/z 41.05 27.03% (I 5000 85

239 •nZz-> j XL l X j +i 169 1 310 352 TT-p- •'rI•<1'I“i•<1'11>111 < 1} 11 TTyTTT-TJTrrTTp-TTTyTTT-TpT-rTYrTTT^^ I' ' ' ' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'I 32.40 32.60 32.80 33.00

22544.D NP091101.M Mon Oct 01 12:59:08 2001 Page 5

' NYC-WTC_06b086926

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NYC-WTC_000086926Source: NYC Law Department, mirrored locally

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