GCMS analysis comments for sample AD28677, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0401\28677.D Vial: 13 Acq On 5 Dec 2001 12:05 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Docosane Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

29.55 0.97 ug/1 211568 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Docosane 310 C22H46 000629-97-0 94 2 Octadecane 254 C18H38 000593-45-3 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 2670 (29.553 min): 28677.D (-) m/ Z 57.00 100.00% 57 43 71 85 5000 — — । । i r । r । i 99 41 JO60 4 j 131—141 155 169182 197 211 239 310 29.20 29.40 29.60 29.80 TTTTTTTTTTT-TrrT‘‘‘t0"‘—ITXIIIT_IIIT‘TTTTTITLTTt7IrII m/z 71.05 73.59% miz-> 40 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72997: Docosane — 43 57

71 5000 85 29.20 29.40 29.60 29.80 m/z 4 3.05 72.91% —I— 99 113127 ■r • । । * । 155169183197211 I ' ' • ' I i ’ ‘ ’ i 292 310 i ■ ■ ■ ■ i' ■ ■ ■ i miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71561: Octadecane 57 43 1 71 1 1' 1 29.20 29.40 29.60 29.80 85 5000 m/z 85.00 53.14% I 99 113 127 141 155 .... - 224 254 T"TCET-IIITE‘TIO"TCIT"‘IIT"SSIT"IVLT""CATOTTITTTIII TTT miz-?.____ 40__ 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71193: Heptadecane ..................I ' ' ' ■ l — । i i i i i r 57 29.20 29.40 29.60 29.80 m/z 41.05 28.12% 71 5000 85

99 _ J J _ 113127 141 155 169 210 240 , — , , , . ----- m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300/77 29.20 29.40 29.60 29.80

28677.D GCMS1126.M Fri Dec 07 15:11:50 2001 Page 2

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