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GC/MS analysis results for sample AD23271, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23271 conducted on October 15, 2001.

NYC-WTC_000088372–000088401

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088385
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23271.D Vial: 19 Acq On : 12 Oct 2001 7:43 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Docosane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 29.62 2.13 ug/1 231749 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Docosane 310 C22H46 000629-97-0 93;^ 2 Octadecane 254 C18H38 000593-45-3 91 3 Heptadecane 240 C17H36 000629-78-7 91^ 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 2678 (29.624 min): 23271 .D (-) m/z SYTOO 100.00% 57 43 71 85 c 553

I 99 29.20 29.40 29.60 29.80 30.00 310 I I 1 i1 I I / I I if I I Ij r IT I I n I I I I I II’. . . r pf I I I I I I 1 I J i ' I ‘ ' I ' ' ' ' I m/z 71.00 72.48% Tlfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72997: Docosane 43 57

552 71 85 u I r7.71 i‘i . |-rr 29.20 29.40 29.60 29.80 30.00 m/z 43.05 69.32% 113127 155169183197211 292 310 iJ I I I'''' r I'' ' ' I '''' ' I''' ' I ' '' ' I 7~rT-rTyT-rT--ry-r-rTT--| ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300

JUa ^bundance #71560; Octadecane 43 5l7

71 29.20 29.40 29.60 29.80 30.00 5000- 85 m/z 85.05 52.27%

113 • 111 11 111 M-Ty+T-T-TYl'T-+TyT4-T-7-[H-T-T-T-yT-T'T-Ty*r-rT-^^ T ' ' ' ' I 7iZz->- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #32063; Heptadecane 7 29.20 29.40 29.60 29.80 30.00 71 m/z 41.00 3^748%

5000 85 J 99

J T’f”' 196 1 ' ' ' ' I ' ' ' ' I T 240 I ' • • ' I « • • ' I ' I ‘ • I ....................................... -n/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80 30.00

23271.D NP091101.M Mon Oct 15 09:37:52 2001 Page 7

NYC-WTC_0b00'88385

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NYC-WTC_000088385Source: NYC Law Department, mirrored locally

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