GC/MS analysis results for sample AD23271, Oct 15 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT12 01\23271.D Vial: 19 Acq On : 12 Oct 2001 7:43 pm Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 6 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

29.50 11.76 ug/1 1276590 Chrysene-dl2 33.12

Hit# Of 5 'entative ID MW MolForm CAS# Qual 1 Butyl hex/decanoate 312 C20H40O2: 000000-00-0 35 2 1-Hexen^ 2-methyl- 98 C7H14 006094-02-6 27 3 Cyclobutane, 1,l-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 4 Cyclop^ntanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 23 Abundance Scan 2665 (29.504 min): 23271 .D (-) Tm/z 56.00 100.00% 50

5000 41 73 129 257 JJl.r 111^.1. 1^157171185199213 j 283 29.20 29.40 29.60 29.80 312 m/z 57.00 47.67% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 50

258 ,,,, 5000 ' ' I ' ' 29.20 29.40 29.60 29.80 73 240 312 129 m/z 43.05 37.66% I t I I''' ‘ I mZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261:1-Hexene, 2-methyl- 50 ..... 29.20 29.40 29.60 29.80 41 m/ z 41.05 37.18% 5000 k 27 70 I I I I I I . I r I I I I I . . . I rr. I I I . . I I ■ > I ■ I > > I > I I I I I I ■ I > I I I I I I I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- , , , I , , , , I , / <-A, , I 5 29.20 29.40 29.60 29.80 m/z 73700 29707% 5000

70

mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23271.D NP091101.M Mon Oct 15 09:37:49 20,01 Page 6

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