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GC/MS analysis results for sample AD22654, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087477
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Docosane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 29.63 1.65 ug/1 256266 Chrysene-dl2 33.13 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Docosane 310 C22H46 000629-97-0 93 \ 2 Octadecane 254 C18H38 000593-45-3 91 ' 3 Eicosane 282 C20H42 000112-95-8 91 . 4 Heneicosane ____________________ 296 C21H44 000629-94-7 91/ Abundance Scan 2678 (29.628 min): 22654.D (-) m7z 57/00 100.00% 57

43 71

5000 85

A •f "' i~^' '

nZz-> 40 JJ 99 lie, ...li .iJ, .1.1 I ' 'I 60 ' I''' ' I ''" ' I ' '' ’ I''I' 80 197211 225239___________ 310 ' i"'.. 11.... I... 11 11.. I.... I.... I. I .. I 100 120 140 160 180 200 220 240 260 280 300 29,20 29.40 29,60 29.80 30.00 m/z 71.05 66.29% Abundance #72997: Docosane

JA 4)3 57

71 5000 -p-T TT-p-r 85 29.20 29.40 29.60 29.80 30,00 m/z 43/00 65.85%

■n/z-> Abundance 40 w 60 80 99 ^]3127 I ‘ ' I ' ' ‘ ' I ' ‘ 155169183197211 292 310 ' I ' ' ' ' I ' ' ‘ ' I ' ' ' ' I ' ' ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I ' ' ' ' I 100 120 140 160 180 200 220 240 260 280 300 A

#71561: Octadecane 57 43 71 29.20 29.40 29.60 29.80 30.00 85 5000 “m/z 85/00 46.76%

99

Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ^bundance #39862: Eicosane 43 5l7 29.20 29.40 29.60 29.80 30.00 71 “m/z 41.05 25.09% 5000 85

I J 99 113127141 155 282 196 240 I'''H i ' '" ' I" ' ' 'I ' I "' H ' ' ' I ‘ ' I T ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80 30.00

22654.D NP091101.M Fri Oct 12 09:09:14 2001 Page 6

NYC-WTC_000087477

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NYC-WTC_000087477Source: NYC Law Department, mirrored locally

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