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GC/MS analysis results for sample AD22654, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087476
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NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File : C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butyl hexadecanoate Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 29.51 5.74 ug/1 889834 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hexadepanoate 312 C20H40O2: 000000-00-0 35 2 1-Hexene, 2'^ethyl- 98 C7H14 006094-02-6 27 3 Cycloheppylamine 113 C7H15N 005452-35-7 27 4 CyclobjXane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 Abundance Scan 2665 (29.509 min): 22654.D (-) m/z 56.00 100.00% 55

5000 41 73 129 257 29.20 29.40 29.60 29.80 283 312 A—A r-p-r-n-p-nrWT m/z 57.00 46.59% TiZz-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #44549: Butyl hexadecanoate A 55

5000 258 JUL 29.20 29.40 29.60 29.80

Ti/z-> Abundance ■p-r-rr-p-r 20 40 u 60 73

80 129 I ' 'I ' ' " I ' 'I ' I I ' ' 1571711?^ ‘ 214 ' p I ' I I lA I , I , . 1 I I

100 120 140 160 180 200 220 240 260 280 300 #1354:1-Hexene, 2-methyl- 240

T 312 m/z 41.00 J 37.04%

5 JU A 41 29.20 29.40 29.60 29.80 5000 m/z 43.00 36.54% 27 I

AA A, 98 p-T-T-rp-T-T-TyT-TTnrpn-T-rTTT-rT-yTTTn-T-TTT-TyT^^ m/2-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #2793: Cycloheptylamine T? 55 29.20 29.40 29.60 29.80 m/z 73.00 29.34% '02 70

Ti/z-> 20 30 ,1 I 40 60 I 84 113 ....... --^-I 80 100 120 140 160 180 200 220 240 260 280 300 1 I ' ' ' ' I 29.20 29.40 29.60 29.80

22654.D NP091101.M Fri Oct 12 09:09:12 2001 Page 5

NYC-WTC_000087476

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NYC-WTC_000087476Source: NYC Law Department, mirrored locally

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