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GC/MS analysis results for sample AD23319, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23319 conducted on October 15, 2001.

NYC-WTC_000088429–000088455

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088441
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23319.D Vial: 21 Acq On : 12 Oct 2001 9:41 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.51 6.43 ug/1 672928 Chrysene-dl2 33.12 Hit# o 5 Tentative ID MW MolForm CAS# Qual 1 Bu 1 hexadecanoate 312 C20H40O2: 000000-00-0 35 2 1 -Hexanediol, 2-ethyl- 146 C8H18O2 000094-96-2 32 3 /-Hexene, 2-methyl- 98 C7H14 006094-02-6 27 4 L-Pentene, 2,4-dimethyl-__________ 98 C7H14 002213-32-3 27 Abundance Scan 2665 (29.509 min): 23319.D (-) m/z 56700 100.00% 55

5000 4' 73 I 129 257 Op . " I 29.20 29.40 29.60 29.80 m/z 57.00 46735% ■n&-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 5

5000 258 ...................... 29.20 29.40 29.60 29.80 240 312 m/z 43.05 39.10% 129 I I 157171185 rTH-pH-rVf-rTV-fyTTH-ryT-TTTYrTVrpH-rTjT-r-^ 214 p ' • ‘ I "U J T)Zz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #8882:1,3-Hexanediol, 2-ethyl- 55

29.20 29,40 29.60 29.80 52 73 m/z 41.05 35.64%

31 103 I I I I * ‘ ' P ' ' ' I I '' ' ' I ' * ’ ' I '' '' I ' ' ' ' I T)/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261:1-Hexene, 2-methyl- lLA 55 29.20 29.40 29.60 29.80 m/z 73700 30.45% 41 152 27 70 98 I ' ' ' ' I ' ' ' ' I ' * ' ' I ' ' ‘ ' I ' ‘ ' I pm-q-m-TT nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23319.D NP091101.M Mon Oct 15 09:49:33 2001 Page 6

NYC-WTC_000088441

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NYC-WTC_000088441Source: NYC Law Department, mirrored locally

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