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GC/MS analysis results for sample AD23319, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23319 conducted on October 15, 2001.

NYC-WTC_000088429–000088455

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088442
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT12 01\23319.D Vial: 21 Acq On : 12 Oct 2001 9:41 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heptadecane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 29.62 1.31 ug/1 136542 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 93^ 2 Hexadecane 226 C16H34 000544-76-3 91 ) 3 Octadecane 254 C18H38 000593-45-3 91/ 4 Octacosane 394 C28H58 000630-02-4 90^ Abundance Scan 2677 (29.619 min): 23319.D (-) m/z 56.95 100.00% 57

43 71

5000 85

99 P"- 113 127 141 29.20 29.40 29.60 29.80 30.00 155 169 183 197 211 tVh- -p-T-r-r-p-rT-T-p-T-TT-YT-T-T-Tn^ • ' I ' ' ' ' I ' ' ‘ ' I “mTz 71710 69.29% Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #71193: Heptadecane 5(7

71 5000 85 29.20 29.40 29.60 29.80 30.00 "mTz 4^700 67.38% 99 .do ............ || ■ Il / „| 127 141 155 169^ , 210............ 240

-n/z->40 60 80 100 120 140 160 180 200 220 240 ‘\bundance #70788: Hexadecane • 57 43 71 29.20 29.40 29.60 29.80 30.00 5000 85 m/z 85.05 46.26%

■nfe-> 40 60 w 80 100 120 140 160 180 200 220 240 I.............. .. p/ \ , I ,, Abundance #71560: Octadecane 43 57 29.20 29.40 29.60 29.80 30.00 “mTz 41.00 27.01% 71 ggw 85

Tl/Z-> 40 60 80 n 100 120 127 141

140 160 169 183 197 210 180 200 220 240 254 I ....................................... 29.20 29.40 29.60 29.80 30.00

23319.D NP091101.M Mon Oct 15 09:49:35 2001 Page 7

NYC-WTC_000088442

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NYC-WTC_000088442Source: NYC Law Department, mirrored locally

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