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GC/MS analysis results for sample AD23498, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.

NYC-WTC_000088774–000088798

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088786
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23498.D Vial: 6 Acq On : 16 Oct 2001 7:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Heptadecane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 29.62 0.98 ug/1 112757 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptadecane 240 C17H36 000629-78-7 91 2 Pentacosane 352 C25H52 000629-99-2 91 3 Octacosane 394 C28H58 000630-02-4 91 4 Octadecane ____________________ 254 C18H38 ' _____ 000593-45-3 91 Abundance Scan 2678 (29.623 min): 23498. D (-) m/z 57700 100.00% 57

85

A/ 5000 4 A I I 113 29.20 29.40 29.60 29.80 30.00 141 169 '' f'' I'''' I I' " • I " '»I " " I " " I' • •»( “mTz 71.00 67762% Tl/Z-> ^bundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 57 #71193: Hepfadecane A 5000 85 - ...... 29.20 29.40 29.60 29.80 30.00 hn/z 43.00 66.97% I I Ft I I I I I fl I H p I I I I I I : I I . 1 I I I H I . I . 1 I rj I I I' * ’' I'''' I nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73718: Pentacosane 43

71 29;20 2a40_2a60L_2930_30W_ 5000 ■m/z 85.05 47.01%

I 99

TTfe-> XU 127 155 183 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 211 I " " I " • • I " • ‘ I ’' " I

Abundance #74211: Octacosane J \ / V A... 43 '29.20~~29.40~29.66~ 29.80 30.00 "Wz 41705 29.16% 71 5000

J 1 , 127 155 183 211 364 T-rp-T yTTVryrTrTYrTTHYrrrTpT-TVpTVrj^rTTT7TT-rTpT-rTynTT^^ ...... ................ TlZZ-> 40 60 80 100 120 140 160 180 200220 240 260 280 300 320 340 360 29.20 29.40 29.60 29.80 30.00

23498.D NP091101.M Thu Oct 18 10:10:39 2001 Page 6

■nYC-WTC_000088786

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NYC-WTC_000088786Source: NYC Law Department, mirrored locally

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