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GC/MS analysis results for sample AD22580, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22580 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087202–000087225

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087215
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22580.D Vial: 8 Acq On : 28 Sep 2001 7:17 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Octadecane Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T. 30.74 0.53 ug/1 94737 Chrysene-dl2 33.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Octadecane 254 C18H38 ’000593-45-3 9)bs 2 Heptadecane 240 C17H36 000629-78-7 91 3 Hexatriacontane 507 C36H74 000630-06-8 91 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91' Abundance Scan 2799 (30.739 min); 22580.D (-) m/z 56795 100.00% 5(7. 43 71 5000 85

nfe-> Abundance 40 a60 80 99

100 120 140 160 180 200 #71561: Octadecane 220 240 260 280 30,40 30.60 30,80 31.00 m/z4370566.35%

5(7 43 71 85 5000 30.40 30.60 30.80 31.00 99 m/z TIToO 65.58% ■tJU I I, T/r-';^^55 , T Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71193: Heptadecane (7

71 30.40 30.60 30.80 31.00 5000 m/z 85.05 47.18% 85

99 J ■'27 141 155 169 210 240 ' I ‘' I' ' I ' ' ' ' I ' ' ' ' I ' ‘ ' I ' ' ' ' I ‘ 40 60 80 100 120 140 160 180 200 220 240 260 280 ' I Abundance #74636: Hexatriacontane 43 5(7 30.40 30.60 30.80 31.00 Tn/z 55.00 25.54%

5000 71 85 J 97 I ‘' I' , 1 211 •nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 30.40 30.60 30.80 31.00

22580.D NP091101.M Wed Oct 03 11:37:49 2001 Page 7

NYC-WTC_000087215

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NYC-WTC_000087215Source: NYC Law Department, mirrored locally

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