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GC/MS analysis results for sample AD22653, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22653 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087303–000087325

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087318
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22653.D vial: 12 Acq On : 28 Sep 2001 11:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Octadecane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 32.77 0.78 ug/1 116242 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 94. 2 Heptadecane 240 C17H36 000629-78-7 91 ) 3 Hexatriacontane 507 C36H74 000630-06-8 91 / 4 Heneicosane ____________________ 296 C21II44 000629-94-7 90 Abundance Scan 3020 (32.767 min): 22653.D (-) m/z 57700 100.00% 5|7

253 85 ~=T==i==i“--T=r{=^^

n/z-> JJ j 50 100 150 200 .... 281.... 250 300 350 400 450 500 32.40 32.60 32.80 33.00 m/z 71.05 63.04% Abundance #71561: Octadecane 57

85 5000 32 40 32.60 32.80 33.00 m/z 43.05 55.67% ,224 254 (1 50 100 150. 200 250 300 350 400 450 500 Abundance #71193: Heptadecane 5|7 1[ 32.40 32.60 32.80 33,00 5000 m/ z 85.05 43.87% 85 fl J/ , 210 240 ... .... .... ......... ' ' I ■nZz-> 50 100 150 200 250 300 350 400 450 500 <\bundance 7 #59136: Hexatriacontane ... ...... b . . .-P-- 32 40 32.60 32.80 33.00____ m/z .55.00 21.21% 5000 85

■nZz-> 50 100 150 200 250 300 350 400 450 500 32.40 32.60 32.80 33.00

22653.D NP091101.M Fri Oct 05 08:56:59 2001 Page 9

NYC-WTC_000087318

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NYC-WTC_000087318Source: NYC Law Department, mirrored locally

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