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GC/MS analysis results for sample AD23324, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.

NYC-WTC_000088316–000088345

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088333
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23324.D Vial: 17 Acq On : 12 Oct 2001 5:46 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Octadecane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.74 6.46 ug/1 732109 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 9L 2 Eicosane 282 C20H42 000112-95-8 91 3 Tetracosane 338 C24H50 000646-31-1 90 4 Heneicosane 296 C21H44 000629-94-7 90 (Kbundance Scan 2908 (31.735 min): 23324.D (-) Wz 57.00 100.00% 57

43 71 85 5000

14 T .A. J j| ,y,^j^^tV^169183197211225239253267281295 338 31.40 31.60 31.80 32.00 m/z 71.00 69761% nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 57 43 71

5000 85 , ./V,V ,,, 31.40 31.60 31.80 32.00 99 m/z4370566.65% 224 I I I 1 . IT I I I I I . I r j . . I I I I I . . I ' I' *' ' I ' ' * ' I I' ‘' r ' ' ' I ' ‘ ' I nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #39862: Eicosane 43 57

71 f T 31.40 31.60 31.80 32.00 5000 85 m/z 85.05 51.15%

II, I 196 240 282 ft n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance 43 57 #73543: Tetracosane AR r' 'T T T 31.40 31.60 31.80 32.00 71 m/z 41.05 26777% 5000 85

99 l| \]^127 155169183197 338 - '294 '' I'' pT-TTp-TT-rpTTTJTT-TTpT-rrp-rTnrp'TTTyTTTTyrTTTp-r^^ 'n/z-«> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23324.D NP091101.M Mon Oct 15 10:33:43 2001 Page 11

NYC-WTC_000088333

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NYC-WTC_000088333Source: NYC Law Department, mirrored locally

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