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GC/MS analysis results for sample AD23324, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.

NYC-WTC_000088316–000088345

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088332
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\OCT1201\23324.D Vial: 17 Acq On : 12 Oct 2001 5:46 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise * r Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Butyl tetradecanoate (myristat Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.64 6.87 ug/1 779184 Chrysene-dl2 33.12 Hit# of 5 Tenferdtive ID MW MolForm CAS# Qual 1 Butyl tetra^canoate (myristate) 284 C18H36O2! 000000-00-0 64 2 OctadecanoZc acid, 2-methylpropyl e 340 C22H44O21 000646-13-9 60 3 Octadecanoic acid, butyl ester 340 C22H44O2i 000123-95-5 40 4 Cyclobujzane, 1,2-diethyl-, trans- 112 C8H16 019341-98-1 27 Abundance /J Scan 2898 (31.643 min): 23324.D (-) m/z 56.00 10^700%

553 4 73 129 285 ,,, , /,vA 340 31.40 31.60 31.80 32.00 "I"" m/z 57.00 53.27% TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 55

553 229 ' ' I ' ' ' ' I ' ' ' ' I ' ' 31.40 31.60 31.80 32.00 211 m/z 43.00 42.65% 284

■n/z-> 40 60 U&Un XJ. I " '' I'''' I 1 Ti 1 I 1 .11 I 1 1 1 11 I 1 11 I

80 100 120 140 160 180 200 220 240 260 280 300 320 340 I''''I

Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 5(7

T T _3t40_Jt60_^t80_3Z00_ 5000 m/z 41.05 36.12% 285 267 J 185 340 I 1 . I . . . 111 I I I I I I I I I I' ‘' I' ‘' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester 5^ f T 31.40 31.60 31.80 32.00 m/z 73.00 31.79%

5000 285 340 73 129 267 185 241 •n/z-> -rp- aW. I' ''' I'''' I'''' I'''' I ' I'''' I I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23324.D NP091101.M Mon Oct 15 10:33:41 2001 Page 10

NYC-WTC_000088332

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NYC-WTC_000088332Source: NYC Law Department, mirrored locally

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