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GC/MS analysis results for sample AD23124, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23124 conducted on October 12, 2001.

NYC-WTC_000088000–000088022

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088014
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NYC 9/11 Public Portal Document

■ Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0401\23124.D Vial: 12 Acq On 5 Oct 2001 2:18 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise : - Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Butyl tetradecanoate (myristat Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.67 2.42 ug/1 493956 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl tetra, banoate (myristate) 284 C18H36O2 000000-00-0 64 2 Octadecanoiz acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 64 3 Octadecan^ic acid, butyl ester 340 C22H44O2 000123-95-5 59 4 Cyclohe: .ne, (1,1-dimethylethyl)- 140 C10H20 003178-22-1 27 ^Msundance Scan 2901 (31.671 min): 23124.D (-) m/z 56.0„0 100.00% 5|B

5000 4 73 129 285 IO 7T 31.40 31.60 31.80 32.00 340 m/z 52.25% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 5S

5000 229 31.40 31.60 31.80 32.00 ? 129 211 284 m/z 43.05, 43.13% ^1^ ! fl 1 ?7 1O1 I, I i'''' I fTi/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance ,448214: Octadecanoic add, 2-methylprapyl ester 57

31.40 31.60 31.80 32.00 5000 m/z 41.0.0 34.85% 285 267 j E ^111 ^29 185 340 - , I 241 I I I ' ‘ ' rrpn m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester . .. 5|B 31.40 31.60 31.80 32.00 m/z 73.0,0 30.82% 5000 285 340

m/z-> 40 60 u 0410. 73 129 185 I 241

80 100 120 140 160 180 200 220 240 260 280 300 320 340 267 k ' ' f 1“^ 31.40 31.60 31.80 32.00

23124.D NP091101.M Tue Oct 09 12:38:01 2001 Page 8

NYC-WTC_000088014

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NYC-WTC_000088014Source: NYC Law Department, mirrored locally

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