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GC/MS analysis results for sample AD23124, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23124 conducted on October 12, 2001.

NYC-WTC_000088000–000088022

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088013
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Lata File C:\HPCHEM\1\DATA\OCT0401\23124.D Vial: 12 Acq On 5 Oct 2001 2:18 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise - Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 7 Hexatriacontane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

30.73 0.99 ug/1 201688 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91' 2 Tetracosane 338 C24H50 000646-31-1 90 3 Eicosane 282 C20H42 000112-95-8 90 4 Heptadecane 240 C17H36 _ 000629-78-7 90' Abundance Scan 2798 (30.725 min): 23124.D (-) m/z 57.0,0 100.00% 57 71 43 5000 85

99

'n/z-> XiXi 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 m/z 30.40 30.60 30.80 31.00 71.00 70.30% Abundance #74636: Hexatriacontane 43 5 7

71 5000 /[ ' ' ' I 85 30.40 30.60 30.80 31.00 QO m/z 43.05 63.36% I .. .L .(I. .\i^.''.F^ltl?^?ff.^^3197211 .1rrTp-TT-TYr'rTprr*rT-TYT-rTTp-rTT^^ i »Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane i 43 57 71 T i I 30.40 30.60 30.80 31.00 ■ i 85 5000 m/z 85.05 49.48% 99 i ,i 155169183197 294 338 ' I ' '' ' I ' * ' ' I' ' ' ' I ' ' ' ' I ' ' I ' p-n-ry I'' ’' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #72326; Eicosane ' /_< I 5(7 30.40 30.60 30.80 31.00 43 m/z 41.0,5 27.08% 71 5 85 99 J 113127141155169 282 '' I' ' I ' ‘ T' I ' ‘ ' I ' ‘ ' I ' ' ' ' I ' I'''' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00

23124.D NP091101.M Tue Oct 09 12:37:52 2001 Page 7

NYC-WTC_000088013

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NYC-WTC_000088013Source: NYC Law Department, mirrored locally

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