Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On : 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample : 9/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 13 Hexatriacontane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 32.76 1.29 ug/1 208771 Chrysene-dl2 33.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Tetracosane 338 C24H50 000646-31-1 90 3 Eicosane, 10-methyl- 296 C21H44 054833-23-7 90 4 Pentacosane 352 C25H52 000629-99-2 90 Abundance Scan 3019 (32.759 min); LBE.D (-) m7z 57700 100.00% 57 43 71
5000 85
32.40 32.60 32.80 33.00 in/z 71710 72.45% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636; Hexatriacontane 43 57
5000 71 85 n- J 32.40 32.60 32.80 33.00 m/z 43.00 69754% J_T ^121?^141155169183197211 T n I " I I ( I I I , I u 1 I I n^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543; Tetracosane 43 57 71 ' I ' ' ' ' I ' A 32.40 32.60 32.80 33.00 5000 85 WZ 85.05 49.86%
99 294. 338 ''' I' I''''I'• '''1' I • ' ’ 'P TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42197; Eicosane, 10-methyl- 57 32.40 32.60 32.80 33.00 43 m/z 41.05 25797% 71 5000 85
I 11 P . . . I r. . . I . . n 1 • • « « P '' ’ I ‘ n'''' I'''' I • *'' r*''' I' ’ > 11'' f I > > > 11 > Tl/Z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 3240 32.60 32^80 33.00
LBE.D NP091101.M Wed Oct 03 14:41:22 2001 Page'13
NYC-WTC_000087150
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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NYC-WTC_000087008
Technical form recording liquid-liquid extraction parameters including drip rates and pH measurements for WTC samples.
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NYC-WTC_000087013
Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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NYC-WTC_000087022
Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.
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NYC-WTC_000087044
Laboratory report documenting GC/MS analysis of sample AD22550 conducted on September 27, 2001, identifying unknown compounds.
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