Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBE. D Vial; 5 Acq On 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample 9/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Tetracosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.77 1.34 ug/1 217032 Chrysene-dl2 - 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Tetracosane 338 C24H50 000646-31-1 91' 2 Heneicosane 296 C21H44 000629-94-7 91 3 Pentacosane 352 C25H52 000629-99-2 91 4 Octadecane 254 C18H38 000593-45-3 87 Abundance Scan 2911 (31.768 min); LBE.D (-) m/z 57700 100.00% 57 I 43 71 85
. ;vL.. . 5000
99 31 40 31.60 31.80 32.00 1 Jil psi 69183197211225239 267281 m/z 71.00 70.09% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71
5000 85 .... MU 31 40 31.60 31.80 32.00 99 1,- m/z 43.00 65.56% I I ll,T? 155169183197 338 294 ' 'I ' TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 71 85 31.40 31,60 31.80 32.00 5000 m/z 85.05 50.42% 99
pT^p-TrTTYrT^Tqp-Wph-TTVpnrTTpT-TT-p-rTpnTTT-p-rTT-pTTTTq^ Ti/z-> Abundance 40
43 57 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73718: Pentacosane .... a/.U..... . 31 40 31.60 31.80 32.00 m/z 41.05 24.67% 71 5000 85
1 II ^1^pi 27141155169183197211225 A-ry'^rT^YrT^TYTV-rTqH-rTYp-TT-TYrTnT-pTTT-p-TT^ Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00
LBE.D NP091101.M Wed Oct 03 14:41:20 2001 Page 12
NYC-WTC_000087149
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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Technical form recording liquid-liquid extraction parameters including drip rates and pH measurements for WTC samples.
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Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22550 conducted on September 27, 2001, identifying unknown compounds.
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