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GC/MS calibration data sheet for October 5, 2001

Machine-extracted title · confidence 90%

Laboratory data sheet listing extraction dates and calibration results for deuterated standards.

NYC-WTC_000087980–000087999

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000087989
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NYC 9/11 Public Portal Document

’Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0401\LB. D Vial: 9 Acq On 4 Oct 2001 11:22 pm Operator: 209 GALOS Sample 9/24 Inst : GC/MS 209 Mise : ■ Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Tetracosane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

29.65 0.70 ug/1 120513 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 90Y 2 Octadecane 254 C18H38 000593-45-3 9OX 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 86 4 Heptadecane 240 C17H36 000629-78-7 86 Abundance Scan 2680 (29.646 min): LB.D (-) m/z 56.95 100.■‘00% 57

43 71 85

29.40 29.60 29.80 30.00 m/z 68.34% mte-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71

5000 85 29.40 29.60 29.80 30.00 99 m/z 4; .05 65.33% i y ll 155169183197 294 338 ‘' I'''' I' I ' ' ' ' I ' ‘ ' I <n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^Abundance #71559: Octadecane 43 57 T i 29.40 29.60 29.80 30.00 lililil 85 m/z 85.05 46.06%

1)3127141155169183 226 254 -T-p-TTTq-rVTTqH-T-Tn-p-rT-TY^ I' • 1111,,. I P" 'n/z-> 40 60 80 100 120 • 140 160 180 200 220 240 260 280 300 320 340 Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl- . I\ 29.40 29.60 29.80 30.00 71 m/z 41.05 26.90% 5000 85

T 183 211 m/z~> X 268 296 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 I'''' I'''' 11 29.40 29.60 29.80 30.00

LB.D NP091101.M Tue Oct 09 12:50:46 2001 Page 4

NYC-WTC_000087989

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NYC-WTC_000087989Source: NYC Law Department, mirrored locally

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