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GC/MS analysis results for sample AD23501, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.

NYC-WTC_000088853–000088879

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088870
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23501.D Vial: 9 Acq On : 16 Oct 2001 10:03 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Tetracosane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.73 3.57 ug/1 399729 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Tetracosane 338 C24H50 000646-31-1 99 2 Eicosane 282 C20H42 000112-95-8 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Heptadecane ____________________ 240 C17H36 000629-78-7 91 Abundance Scan 2908 (31.734 min): 23501 .D (-) m/z 57700 100.00% 57 43 71

M 5000 85-

31.40 31.60 31.80 32.00 338 m/z 71710 70.59% nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 5Z 71

5000 85 31.40 31.60 31.80 32.00 m/z 43705 67724% I J il T’F I . I I . IT I I I I . . I 1 I I . I 155169183197 p-rrVp-f-rryVTT-fp 338 p 294 I'''' 1 ‘ Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #39862: Eicosane _43_57

71 31.40 31.60 31.80 32.00 5000- 85 m/z 85.05 47.76%

I I ^1131^1411^ 196 240 282 1 I'''' I'' I ' '' ' I ' I ' ' ' ' I ' ' '' I

®ibundance 40 57 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #71561: Octadecane ..... zs/U..... 31.40 31.60_31.80 32.00 -143 71 Tm/z 4 It. .05-- 26764% 85 5000

224 ^ ' I ' ' ' ' I ' ‘ I ' ' ' ' I ' '' ' I t• ''’I' I""1 I '~’T Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23501.D NP091101.M Thu Oct 18 10:21:43 2001 Page 11

NYC-WTC_000088870

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NYC-WTC_000088870Source: NYC Law Department, mirrored locally

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