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GC/MS analysis results for sample AD23843, Nov 2 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23843 conducted on November 2, 2001, identifying unknown compounds.

NYC-WTC_000089397–000089417

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089412
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23843.D Vial: 15 Acq On : 31 Oct 2001 4:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : ' Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************************************************* * * ******************. Peak 'Number 8 Tetracosane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

31.68 1.73 ug/1 428776 Chrysene-dl2 33.06

Hit# of 5 Tentative ID MW MolForm CAS#

1 Tetracosane 2 Eicosane 338 282 C24H50 C20H42 000646-31-1 {^9/ 000112-95-8 9i 7) 3 Octadecane 254 C18H38 000593-45-3 91 4 Heneicosane ____________________ 296 C21H44 000629-94-7 91 flibundance Scan 2902 (31.684 min): 23843.D (-) Wz 57.00 100.00% 57

43 71 85 5000

' ' I' ' ' ' I I

Tife-> Abundance LLO 40 60 . 39 113 . ,V.

80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■' I" " f ■ ■ m/z 31.40 31.60 31.80 32.00 71.05 69.81% #73543: Tetracosane 43 57 71

5000 85 - 31.40 31.60 31.80 32.00 m/z 43.05 66.18% 11.:* . . . .1 ■ .'1 ■ j ..... ........... , nZ2-> 40 60 80 100 120 140 160 180 ^0 240 260 2^ 300 320" Abundance #39862: Eicosane “43-5(7

71 5 31.40 31.60 31.80 32.00 f>T-i-r-p-r

5000 85 m/z 85705^ 50.26%

_|_|-gj^113127141155 282-- I I I I T I I "| I I r I I ri I I f I I I I I 196 ------ 240 ''' I ‘‘ I'' •' p • ' I'''' I Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 57- . — 31.40 " 31.60'31.80-732.00—- -43- "m/z 41.05 26723% 85 5000

nfe-> '' I'' 40 60 99

I I n I I T I I I I I I r I I rm । ■ ■ ■ ■ । । ■ 80 100 120 140 160 180 200 220 240 260 280 - 300 320 340 .224....^.........--■7. ' r ''' I' ’'' r ''' P ' /' 1'''' I'' ' I'' M' I ' ' ' 31.40 31.60 31.80 32.00

23843.D NP103001.M Thu Nov 01 14:45:01 2001 Page 8

NYC-WTC_000089412

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NYC-WTC_000089412Source: NYC Law Department, mirrored locally

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