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GC/MS analysis results for sample AD23843, Nov 2 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23843 conducted on November 2, 2001, identifying unknown compounds.

NYC-WTC_000089397–000089417

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089411
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23843.D Vial: 15 Acq On : 31 Oct 2001 4:11 am Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS' 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Butyl tetradecanoate (myristat Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

31.59 1.15 ug/1 285407 Chrysene-dl2 33.06

Hit# of 5' Tentative ID MW MolForm CAS# Qiial

1 Butyl tetradec^oate (myristate) 284 C18H36O2 000000-00-0 '59 2 Octadecanoic/acid, butyl ester 340 C22H44O2 000123-95-5 45. • 3 1 - Pent ene, 4-dimethyl- 98 C7H14 002213-32-3 27 • 4 l-Hexene,/2-methyl-_______________ 98 C7H14 006094-02-6 ~27 Abundance Scan 2892 (31.593 min); 23843.D (-) m/z 56.00 100.00% /Y

5000 4' 73 285 157 , If® 213 241 267 j 340 31.20 31.40 31.60 31.80 32.00 “TTYttTTJ-rrTTjTTrTp^TTTyrrTVp^TT-pS^^ m/z 57.00 48.65% ttZz-> Abundance 20 40

53 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #40186; Butyl tetradecanoate (myristate) fl 5000 229 31.20 31.40 31.60 31.80 32.00 ^73 129 211 m/z 43705 39.63% 284 T I I ’''' I ‘' I''' ' I ' "'' I'' ' ' I I J " . I . 11 r 11 ,. , I Ti^-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester 3 MU 31.20 31.40 31.60 31.80 32.00 5000 mZz 41.05 36767% 285 340 7 129 185 267 I ■ 241---- 1------ ttZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #63263; 1 -Pentene, 2,4-dimethyl- ------------------------------- gt- ------- -------------- ----- ---------------------- —-- ---------------------------------- -------- ------------ sa_ ------- ,---------- ------------------------------------------- ---------- --------.—----- ------—---------------------------——- 31.26<3t46-31.^ 31.80'32.66’ 777 55707 30.84% 5000 4 (1 , 83 98 iTi I . . I. I .. . rp •.. I .... I ... k I .... I ...... '" I'" ‘I I ‘ ‘' I vfz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.20 31,40 31.60 31.80 .32.00

23843.D NP103001.M Thu Nov 01 14:44:51 2001 Page 7-

NYC-WTC_000089411

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NYC-WTC_000089411Source: NYC Law Department, mirrored locally

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