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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089324
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT3001\23799.D Vial: 10 Acq On : 30 Oct 2001 11:19 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Butyl tetradecanoate (myristat Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.59 1.17 ug/1 '331615 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl tetradecan^te (myristate) 284 .C18H36O2: 000000-00-0 64 2 Octadecanoic acia, butyl ester 340 C22H44O2! 000123-95-5 45 3 2-Methyl-N-l-t/rdecene 196 C14H28 018094-01-4 27 4 1-Hexene, 2-methyl- 98 C7H14 . 006094-02-6 27 Abundance Scan 2892 (31.591 min): 23799.D (-) m/z 56.00 100.00% 53

5000 4‘ 73 I Q7 129 285 340 31.20 31.40 31.60 31.80 32.00 m/z 57.00 49.80% nfe-> . 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 53

5000 229 31.20 31.40 31.60 31.80 32.00 73 211 iriTz 43.05 38.98% 129

nfe-> 1 I''' ‘ I'''' 20 40 60 60 100 120 140 160 180 200 220 240 260 280 300'320•340' I'''’I 284 ' I I ''' I I'

Abundance-------------------------------- #73570: Octadecanoic acid,-butyl ester---------- —r 5

' ' I ' ' .31.20 31.40 31.60 31.80 32.00 5000 m/z 41.00 32.62% 285 340 73 267 129 185

TiZz-> 20 40 4^ aXiX 60 I ' 'I '‘ 'I‘'r 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #21975:2-Methyl-N:14ridecene , __ •"-fr, r/ I I I ,• ----53 -31.20 -31-40--31.60 -31:80-32;00- ■Wz 7^700 31.86%

5000

27 I 83 ,,, I I 1 140 168 1^ I ' • ' ' I• •1 'I ' I'•HI I ' ' • I I ' ' i^^T'r p. I T . 1 . . I'' " I'' I" " i"' " I' ' I " '' I' " ' I'' " I " ' 11' Tlfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.20 31.40 31.60 31.80 32.00

23799.D NP103001.M Thu Nov 01, 13:16:48 2001 Page 7

■“NYC-WTC_OOOO89324

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NYC-WTC_000089324Source: NYC Law Department, mirrored locally

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