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GC/MS analysis results for sample AD22580, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22580 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087202–000087225

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087216
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NYC 9/11 Public Portal Document

Library Search Compound Report I

Data File : C:\HPCHEM\l\DATA\SEP2801\22580.D Vial: 8 Acq On : 28 Sep 2001 7:17 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************* *’ * **********

Peak Number 8 Butyl tetradecanoate (myristat Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 31.68 0.97 ug/1 173899 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl tetrajaecanoate (myristate) 284 C18H36O2 000000-00-0 53 . 2 Octadecam ■ic acid, butyl ester 340 C22H44O2 000123-95-5 40 3 1-Hexene 2-methyl- 98 C7H14 006094-02-6 27 4 Cyclohe^:ane, (1,1- dimethylethyl) - 140 C10H20 003178-22-1 27 Abundance Scan 2901 (31.675 min): 22580.D (-) m/z 56.00 100.00% 55

5000 4 73 129 285 Ha il I 97 185 31.40 31,60 31.80 32.00 241 T 1 rr/ri I I I rt-rr|-Fi i i । 340 rrb. m/z 57.00 49.81% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 55 I

5000 T T V 229 31.40 31.60 31.80 32.00

Wz-> Abundance 20 40 60 u73 129 211 I I'''' I'' ‘' I' I'' I'''' I 80 100-120 140 160 180 200 220 240 260 280 300 320 340 #73570; Octadecanoic acid, butyl ester 284 ' J ''' I'''' I ‘' I mA 43705 46.23%

55

31.40 31.60 31.80 32.00 5000 m/z41.05 38.84% 285 340 267 185 I Y I " I " '' I'' " I " " I' " ' I " '' I' " ' I '' I' " ' I'' ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #1354; 1-Hexene. 2-methyl- 50 31.40 31.60 31.80 32.00 mA 55.00 32.07% 41 5000

,1 83 ^1^ ' I''' ' I' r ''' I ’''' I I " '' I " " I " '' I' " ' I " '' i T T Tife-> 20 40 60 80 100 120 140 160 180 200 220 240260 280 300320 340 31.40 31.60 31.80 32.00

22580.D NP091101.M Wed Oct 03 11:37:51 2001 Page 8 J NYC-WTC_000087216

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NYC-WTC_000087216Source: NYC Law Department, mirrored locally

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