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GC/MS analysis results for sample AD23323, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23323 conducted on October 15, 2001.

NYC-WTC_000088290–000088315

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088306
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23323.D vial: 16 Acq On : 12 Oct ,2001 4:47 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 10 Butyl tetradecanoate (myristat Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.65 2.80 ug/1 288970 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl tet;?adecanoate (myristate) 284 C18H36O2: 000000-00-0 64 2 Octadecaiioic acid, butyl ester 340 C22H44O2; 000123-95-5 59 3 Octadit^anoic acid, 2-methylpropyl e 340 C22H44O2: 000646-13-9 46 4 Cycl/^ipropane, 1-(1-methylethyl)-2-n 210 C15H30 041977-39-3 27 <\bundance Scan 2898 (31.647 min): 23323.D (-) Wz 56.00 100.00%

T 5000 4 73 I ^2® 285 I JJ i- 143157171'1^^199213227241 340 _3t40_31J0_3t80_JZ00_ (Tf i Til |T I 11 I 1 11 T I i'. I I J 'i I I I J I I 'i I I . . I • p I I I I T I I I j I I m/z 57700 50.27% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 55

5000 229 31.40 31.60 31.80 32.00 211 m/z 43705 43.06% 284 §7101 I I T T TL TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester 55

31.40 31.60 31.80 32.00 5000 m/z 41.05 39.73% 285 340 73 129 267

■n/z-> 40 ' ‘ I' ■iL 60 185 I r ‘' I'''' I'''' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 241 I •T-pn xXt Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57 31.40 31.60 31.80 32.00 m/z 73700 31.29%

5000 285 207 I 241 [ I 340 T I I I i''i I I I kT I ry I r I I I Y^H-rTyTTTTyTTTT-^TTTTyrJt-rTyTTT-^ Tlfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23323.D NP091101.M Mon Oct 15 10:29:35 2001 Page 10

NYC-WTC_000088306

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NYC-WTC_000088306Source: NYC Law Department, mirrored locally

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