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GC/MS analysis results for sample AD23323, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23323 conducted on October 15, 2001.

NYC-WTC_000088290–000088315

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088305
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23323.D vial: 16 Acq On : 12 Oct 2001 4:47 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209' Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 9 Heneicosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 30.70 1.33 ug/1 137161 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 Heneicosane 296 C21H44 000629-94-7 9 2 Tetracosane 338 C24H50 000646-31-1 9 3 Octadecane 254 C18H38 000593-45-3 87 ■ 4 Tricosane ____________________ 324 C23H48 000638-67-5 87 ^bundance Scan 2795 (30.702 min): 23323.D (-) m/z SYTOO 100.00%

43 57

71 I 5000- 85

.1. 99 |] \^^'?^'41155169183197211 J. T’-'-m- 30.40 30,60 30.80 31.00 [Ti I / [ . . T. I I I I I fi I i"i I . 1 . I I I 1 . I I 1 1 . . I iTI'rr'ph- .. I .... I I > I I I I . I I I m/z 71.00 68.03% n/z-> Abundance 40 60 80 100 1 20 140 160 180 200 220 240 260 280 300 320 340 #42201: Heneicosane I 5f7 71 85 aga 30.40 30.60 30.80 31.00 m/z 43.05 63.07% 113- '''27141155 I 268 296 p-r-rr-p-rr-tp I ’ ' ' ' I ' ' ' I ' ’ ' ' I ' ' ' ' I ' ' ' ' I r ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 5t7 71 m pii-/ ri r| t r 30.40 30.60 30.80 31.00 5000- 85 m/z 85.05 49.58% I

n/z-> 40 JJ 99,.o p-| I I |Ti 1 « I I .1 I I ... I I 60 155169183197 80 100 120 140 160 180 200 220 240 260 280 300 320 340 r'''I 294 I ’ ' ' ’ I 338

Abundance #71560: Octadecane 43 5(7 30.40 30.60 30.80 31.00 m/z 41705 25.88% 71 5000 85

J 169183197 254 I'''' I Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00

23323.D NP091101.M Mon Oct 15 10:29:33 2001 Page 9

NYC-WTC_000088305

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NYC-WTC_000088305Source: NYC Law Department, mirrored locally

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