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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089325
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NYC 9/11 Public Portal Document

Library' Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23799.D Vial: 10 Acq On : 30 Oct 2001 11:19 pm Operator: 209 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library : C;\DATABASE\NBS75K.L ************************************************* * * ****************** Peak Number 8 Heneicosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.68 1.17 ug/1 332832 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91'^ 2 Tetracosane 338 C24H50 000646-31-1 91 3 Pentacosane 352 C25H52 000629-99-2 91 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44. 054833-48-6 91" Abundance Scan 2902 (31.682 min): 23799.D (-) m7z 57.00 100.00% 5(7

43 71 85 5000

®®113 31.40 31.60 31.80 32.00 ' m ‘" I •''' I' m/z 71.10 68.34% nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 71 85 5000 31,40 31.60 31,80 32.00 99 m/z43.05 64.02% 268 296 J I IJ I I r» I I j I IT t I I I I I I I I I « I I ' ' ' ' I ' ’ ' ' I T'' " I' " ’“P nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543; Tetracosane 43-57----- 71 ' ' ' I ' ' ' ' I ' ' rnTY-r'. T I Ti ■ - 31.40 31.60 31.80 32.00 5000 85 m/z8570^ 50.66%

99 ........ .................. ! , , ,1 , , ( , , ,ll, . ............... .......... -,■^-7........7?^ TTfe-> 40 60 80 100 120 140 160 180 :ao 240 2TO 2^ 300 320 Abundance #73718: Pentacosane 31.40 -31.60-31.80 -32.00- -m/z—41-i-O 5—23-.-5-9 %

7-Jfc 71 5000 85

I 1 I I I T. . , I . . . . I , , ,I , , , , I , . , , I , , , , I , , , , I "T* P ’ ' ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23799.D NP103001.M Thu Nov 01 13:16:51 2001 Page 8

NYC-WTC_000089325

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NYC-WTC_000089325Source: NYC Law Department, mirrored locally

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