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GC/MS analysis results for sample AD23318, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23318 conducted on October 15, 2001.

NYC-WTC_000088402–000088428

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088416
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23318.D Vial: 20 Acq On : 12 Oct 2001 8:42 pm Operator: 209 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Heneicosane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 30.71 2.00 ug/1 212037 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 9L 2 Octadecane 254 C18H38 000593-45-3 91X 3 Tetracosane 338 C24H50 000646-31-1 90 / 4 Docosane 310 C22H46 000629-97-0 87^ Abundance Scan 2796 (30.706 min): 23318.D (-) m/z 57.00 100.00% 57 43 71

5000 85

30.40 30.60 30.80 31.00 m/z 71.00 70.75% m/2-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #42201: Heneicosane J 57 71 85 5000 30.40 30.60 30.80 31.00 99 m/z 43.00 6^/51% 268__ 296 ■I''“' I'''' I'''' I 11 ■ 111" 11,, nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71560: Octadecane 43 57 .......... I ' ' ' t 71 30.40 30.60 30.80 31.00 5000 85 m/z 85.05 49.63%

99 J '']3127i41 169183197 254 '" ' I ’' ' ' I ' ' *' I ' ' ’ ' I ' ' ' ' I ' ''' ' I' ' ' '' I ' ' ' ' I '''' I p-rrrprrTT-T ■Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 30.40 30.60 30.80 31.00 71 m/z 41.00 25.70% 5000 85

1- jlW' 155169183197 294 I '' " I' ''' I''''' I ''' ' I'''' I " '' I' " ‘ I'''' I'''' I'''' I''' ' I ‘ 338 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00

23318.D NP091101.M Mon Oct 15 09:45:56 2001 Page 8

NYC-WTC_000088416

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NYC-WTC_000088416Source: NYC Law Department, mirrored locally

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