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GC/MS analysis results for sample AD23321, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23321 conducted on October 15, 2001.

NYC-WTC_000088237–000088262

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088254
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23321.D Vial: 14 Acq On : 12 Oct 2001 2:50 pm Operator: 209 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Heneicosane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 32.73 2.74 ug/1 344525 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91- 2 Octadecane 254 C18H38 000593-45-3 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 3016 (32.731 min); 23321 .D (-) m/z 57.00 1WTOO% 57

5000 85

4- 32.40 32.60 32.80 33.00 141 169 196211 238253 281 352 ^T' ' P ‘' I' " ' I ’ " ' I' • ” I' " ' I " '' I ’' " I ’ " ’ I " '' I m/z 71.00 72.86% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #42201; Heneicosane 7

S3 85 T Jx 32.40 32.60 32,80 33.00 m/z 43.05 tt-t

66.74% '' I ‘ 44 I " «' I " " I'' • ’ I " ' • I 268 296 I' " ' I " ' 11' J ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561; Ocladecane 7

32.40 32.60 32.80 33.00 85 253 m/z 85.05 48.61% I 224 ■ I " '' I'' " I * I'''' r * ‘' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #39862: Eicosane ....................................... - 32.40 32.60 32.80 33.00 Wz 41.05 25.03% 5000 85

282 240 196 I'''' I' 'I' ’ I'' " I'' •' I " • • I ' ‘ I ' ''' I •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

23321.D NP091101.M Mon Oct 15 10:22:34 2001 Page 10

NYC-WTC_000088254 '

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NYC-WTC_000088254Source: NYC Law Department, mirrored locally

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