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GC/MS analysis results for sample AD23502, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23502 conducted on October 19, 2001.

NYC-WTC_000088880–000088904

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088898
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

'Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23502.D vial: 10 Acq On : 16 Oct 2001 11:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Heneicosane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 33.69 3.25 ug/1 381626 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 9I< 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91 > 3 Eicosane, 9-octyl- 394 C28H58 013475-77-9 91 / 4 Hexatriacontane 507 C36H74 000630-06-8 93/ Abundance Scan 3120 (33.686 min): 23502. D (-) m/z 57700 100.00% 57

85 5000

33.40 33.60 33.80 34.00 169 197 239 281 366 OA ' I'' ‘' I' " U ' ‘' I ‘" I'''' I " " I'' '' I' ''' I' " ' I " '' I' " ' I' " ' I ‘ m/z 71.10 71.19% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #42201: Heneicosane 57

85 5000 T 33.40 33.60 33.80 34.00 Wz 43.05 66783% I 113 jbuUuXvr 268 296 I•'"I""I""I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 ^bundance #50999: Eicosane, 7-hexyl- S|7. Ik p'' n 33.40 33.60 33.80 34.00 5000 85 m/z 85.05 50.88%

182 281 310 I I'''' I " pTTTpTTTjrTTTfTTrrpTTTY T’ ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #53460: Eicosane. 9-octyl- I7 43 - 33.40 33.60 33.80 34.00 -mAz-— 55.00 26.08% 71 5000

QQ 281 I II il I t 352 394 pT^TjtTTTYrrVTp-HTfTTTYpTTTpTTTpTTTyrTTTYrTTrp-rTTfrTTTpTTTpTTrrpT^^ •nZz~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 33.40 33.60 33.80 34.00

23502.D NP091101.M. Thu Oct 18 10:25:06 2001 Page 12

NYC-WTC_000088898

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NYC-WTC_000088898Source: NYC Law Department, mirrored locally

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