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GC/MS analysis results for sample AD23319, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23319 conducted on October 15, 2001.

NYC-WTC_000088429–000088455

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088449
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23319.D Vial: 21 Acq On : 12 Oct 2001 9:41 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Heneicosane, 11-(1-ethylpropyl Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.60 3.16 ug/1 329999 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91 3 Hexatriacontane 507 C36H74 000630-06-8 91 4 Eicosane 282 C20H42. 000112-95-8 91 Abundance Scan 3220 (34.604 min): 23319.D (-) m/ Z 57.00 100.00% 7 71 43 5000 85 I ■p“

34.20 34.40 34.60 34.80 35.00 T-q-r-r-r-r-f-r-T m/z 71.00 70.42% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #51002: Heneicosane, 11 -(1 -ethylpropyl)- 43 57

71 553 85 34.20 34.40 34.60 34.80 35,00 m/z 43.05 65.23% I 1 183197211225 295 333 TT^pT’VTT^H-TYYrT^TpVrTqH-TTTyTTTTj'rrTT'yrrTTpVTTpn-rTjTTrTp-rTVpT-TT^^ nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #50999: Eicosane, 7-hexyl- 43 57

T 71 34.20 34.40 34.60 34.80 35.00 553 85 mTz 85.05 47.24%

I \]3127i41 281 310 ... T rp-rnCpi . ■ . । . . ■ ■ । IT' I l 1111111 ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Hexatriacontane 43 5 7 34.20 34.40 34.60 34.80 35.00 m/z 55.00 23.82% 71 5000 85

L 69183197211 r ' ' ' I ' ' ' ' I ' ' ' ' I '' ' ' 1' ' ' ' I 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.20 34.40 34.60 34.80 35.00

23319.D NP091101.M Mon Oct 15 09:49:51 2001 Page 14

NYC-WTC_000088449

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NYC-WTC_000088449Source: NYC Law Department, mirrored locally

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