NYC-WTC_000035153
Laboratory report noting TurboVap contamination and recovery data for sample AD28663.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 17 pages
GCMS analysis comments for sample AD28678, Dec 2001
Machine-extracted title · confidence 100%Laboratory report noting TurboVap contamination and low recovery rate for sample AD28678.
NYC-WTC_000035072–000035088Folder label: “GCMS X 11/24/01 A 12/4/01”
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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28678.D Vial: 16 Acq On 5 Dec 2001 3:01 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heneicosane, 11-(1-ethylpropyl Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.
32.66 1.11 ug/1 206783 Chrysene-dl2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qu 1 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 2 Eicosane, 9-octyl- 394 C28H58 013475-77-9 91 3 Tetracosane 338 C24H50 000646-31-1 90 4 Octadecane, 2-methyl- 268 C19H40 001560-88-9 90 Abundance Scan 3008 (32.656 min): 28678.D (-) m/z 57.00 100.00% 57
5000 85
. , .1 11 113 141 . 169 197 225 253 281 32.40 32.60 32.80 33.00
m/z-> IX 40 60 TTTTTTTTTT) m/z 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 43.05 74.07% Abundance #51002: Heneicosane, 11 -(1 -ethylpropyl)- 43
71 5000 --32.40 ---- P- 32.60 32.80 33.00 m/z 71.00 66.90% I 99 LL127183225293 TTI"n—TT—TITTOTTTTTTTETTTTT .. n I n h (i. "I0‘TETT"TTTTETTTTTTT miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #53460: Eicosane, 9-octyl- 43 — T . —1 71 32.40 32.60 32.80 33.00 5000 m/ Z 85.05 46.63%
qq 281 1127 155............ 238 "P " TTTCI—U010——0T"TETTTIUTTTTT । ..... 7.......... ,352 .... 394 , T"TVIETTTTETTETTTCE‘ICETTTTTTT m/z-> 40 60 80 100 120 140 160 180 2(X) 220 240 260 280 300 320 340 360 380 Abundance 57 #73543: Tetracosane ... 4 — , -A 32.40 32.60 32.80 33.00 m/z 55.00 28.64% 5000 85
m/z—> J 11.155 183...... 294.. 338.... " 1111 TT9———1"Tu—TETT"TEITCTEOCTEITTTTTTTTTTT"TTTCVITVTTTET ‘T‘TTTTTTT‘‘I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 •4* 1 । 1AT 32.40 32.60 32.80 33.00
28678.D GCMS1126.M Thu Dec 06 15:13:46 2001 Page 7
NYC-WTC_000035084
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NYC-WTC_000035084Source: NYC Law Department, mirrored locally
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