GCMS analysis comments for sample AD28678, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28678.D Vial: 16 Acq On 5 Dec 2001 3:01 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Hexadecane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 33.61 1.17 ug/l 219189 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexadecane 226 C16H34 000544-76-3 (97 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91 3 Tetracosane 338 C24H50 000646-31-1 90 4 Heptadecane 240 C17H36 000629-78-7 87 Abundance Scan 3112 (33.611 min): 28678.D (-) m/z 57.00 100.00% 57

71 43 5000 85

--- TPT -PPP I it i r . t

L , L . 1 . ........... . T* TUmmm] 33.20 33.40 33.60 33.80 34.00 m/z 71.10 68.63%

1 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #70788: Hexadecane 57 43 71 1 5000 85 TPT ' ' 1 ' i ‘ ■ i ' ■ ■ ■ i ' ' 33.20 33.40 33.60 33.80 34.00 m/z 43.05 61.80% 99113127141155169183 226 ITT TTIPTT n I > ■■ ■ ■ I ■ I.. ■. I • I ■'' 111111111 111111111111 11 mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #50999: Eicosane, 7-hexyl- 43 57 TfTT TTTTrrmer 71 33.20 33.40 33.60 33.80 34.00 m/z 85.05 43.77% 5000 85

7 113127141 182197 281 310 III’T 1‘ ' I . ' " | ' ' ' ' | | | 1 I' 1 ' | । H . । ! ! ! ! | ! I I I I1 . . . . । . . . TITTT I | I mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 2 43 57 33.20 33.40 33.60 33.80 34.00 71 m/z 55.00 24.88% 5000 85

[ J 113127 155169183197 294 338 1' l‘ • 1’3 1 ■ I T 1 ' | 1 . . .. ! . r. . | i i . . 1 . . , , | I I II I n ri I I I I I I I I I I'| I A Aap । 4 —*-A4*74 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 33.20 33.40 33.60 33.80 34.00

28678.D GCMS1126.M Thu Dec 06 15:13:48 2001 Page 8

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