GCMS analysis comments for sample AD28663, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC0401\28663.D vial: 17 Acq On : 5 Dec 2001 3:59 am Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Heneicosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

30.63 0.98 ug/1 195521 Chrysene-dl2 33.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7/91 2 Eicosane 282 C20H42 000112-95-8 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Pentacosane 352 C25H52 000629-99-2 91 Abundance Scan 2787 (30.626 min): 28663.D (-) m/z 57.00 100.008 57 43 71

5000 85

m/z-> ‘ I 40 □ 1 117141155168 182196210, 60 80 100 120 140 160 180 200 T 2 0 240 260 ITT 280 300 30.20 30.40 30.60 30.80 31.00 m/z43.05 74.67% Abundance #42201: Heneicosane 57 71 85 5000 CI r TT TT T T , TTTTuri 30 20 30.40 30.60 30.80 31.00 99 m/z 71.0.0 73.12% — . ..................................... ........................ .. +1 100 120 140 160 180 200 220 240 260 280 300 miz—> 40 60 80 Abundance #72323: Eicosane 43 57 30.20 30.40 30.60 30.80 31.00 71 m/z 85.05 46.03% 5000 85

‘II _ 1 ITT. . 99 U60yn- ‘ 113 1271111′1 p-rT-rj tt< 141................................ ‘‘ 1 ‘ 11, 11111111111 ‘ 282.... 1′111111/1111111′1111 m/z—> 40 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 57 #71193: Heptadecane fTpr -................— 30.20 30.40 30.60 30.80 31.00 m/z 55.00 26.21% 71 5000 85

— ! | I I 2 .113 127 141 155 169 210 240 I'. | TT . . f. . | ' I | t I ' ' | ' ■ . . |I TITTTTTTTTTTT m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 30.20 30.40 30.60 30.60 31.00

28663.D GCMS1126.M Thu Dec 06 15:31:30 2001 Page 4

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