GCMS analysis comments for sample AD28663, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\DEC0 401\28663.D vial: 17 Acq On 5 Dec 2001 3:59 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Acetic acid, octadecyl ester Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 29.68 0.94 ug/1 186953 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 2 1-Pentadecanol 228 C15H320 000629-76-5 62 3 1-Octadecanol 270 C18H380 000112-92-5 53 4 1-Pentadecene 210 C15H30 013360-61-7 49 Abundance Scan 2684 (29.681 min): 28663.D (-) m/z 43.00 100.00% 43 |

5000 55 69 83 97

l 111

, 125 । 139 153 224 UA... 29.40 29.60 29.80 30.00 m/ Z 83.05 50.80% — , T I | l"l I I '| I I Ihl | I I I I |-I-|-T-|-| I I I I p I I I | I I I I |

m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #73048: Acetic acid, octadecyl ester 43

— PPPP — 1 5000 61 83 97 29,40 29,60 29.80 30.00 "/Z 55.00 45.73% 111 125 139 224 252 ■ ■ i ' ■ ■ i ■ • ■ ■ i ■ ■ • • i ■ > > > । ■ ■ ■ ■ । ■ • ■ ■ । ■ ■ ■ ■ । m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #70846:1-Pentadecanol 69 83 31 97 ----- 29.40 29.60 29.80 30.00 5000 56 111 m/z 60.95 45.24%

LLL i I 125 182 210 t_ 1 1 1 1 1 'Tr

—A. . ■ ■ i ■ ' ■ ■ i ■ ■ ■ ■ i ' • ' ■ i ■ • ' ' i ■ ■ ■ ' I 1 1 1 1 I mlz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #72029:1-Octadecanol TIT 43 55 69 83 29.40 29.60 29.80 30.00 97 m/z 57.00 43.44% 5000 111

n/z-> T-r-p-T-r-r-p-r 40 60 80 100 L 125

120 • ■ । 140 224 252 ■ i ■ • • * i ■ ■ ■ ■ i • > ■ । I 1 1 ■ 1 I 1 1 1 1 I 160 180 200 220 240 -----.......... — 29.40 29.60 29.80 30.00

28663.D GCMS1126.M Thu Dec 06 15:31:27 2001 Page 3

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