GCMS analysis results for sample AD26320, Dec 2001

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Laboratory report of GCMS analysis for sample AD26320 conducted on December 4, 2001.

NYC-WTC_000037104–000037115

Folder label: “GCMS X 12/10/01 A 12/15/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\26320.D Vial: 25 Acq On 16 Dec 2001 1:54 am Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *************************************************** **************** Peak Number 3 Acetic acid, octadecyl ester Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.66 2.29 ug/1 536768 Chrysene-dl2 33.00

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, octadecyl ester 2 1-Heptadecanol, acetate 312 298 C20H40O2 C19H38O2 000822-23-1 000822-20-8 90 (9) 3 1-Octadecanol 270 C18H380 000112-92-5 81 4 4-Tetradecanol 214 C14H30O 001653-33-4 81 Abundance Scan 2682 (29.663 min): 26320.D (-) m/z 43.00 100.00% 43

5000 55 83 69 97

I 111 , ..... J........ , | , di ,||. 125 139 153 168 182 196 224 252 29.40 29.60 29.80 30.00 —d । if it । i । TTTTTTTtr । । f « i fi । । t i • । । TTTTT f r i i'| i'i f । । । । । । । r r i TTT m/z 50.62% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44575: Acetic acid, octadecyl ester 43 57 83 97 5000- 70 T TA-r in 29.40 29.60 29.80 30.00 125 m/z 55.00 49.15% | 208 224 22 282 1 ■ 1 i • ■ ‘ I ' ' ' ’ I m/z--> 40 60 80 100 120 140 160 180 200 220' ‘ 240• 260 280 300 Abundance #42500: 1-Heptadecanol, acetate 43 -P — —PP 83 29.40 29.60 29.80 30.00 5000 61 97 m/ z 57.00 44.84% 111 •: 1: : 125 140 210 238 298 ' ■ I ' ■ I '' ■ ' I ' ' ■ I ■ ■ | ■ ' ■ ' | ■ ■ • ■ | ■ ' • ■ | ■ ■ • • | • ■ ■ > | • .-i-j-i-ri-i-c > i > i | i i i 1 | f m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72029: 1-Octadecanol 43 55 69 83 29.40 29.60 29.80 30.00 97 m/z 60.95 41.28% 5000- 111 125 , , |l L.................... ............. 224 252................... -- — -4 • > i ■ ■ "IT TII" miz—> 40 60 80 1C 120 140 160 180 200 220 240 260 280 300 29.40 29.60 29.80 30.00

26320.D GCMS1126.M Fri Dec 28 13:05:53 2001 Page 3

NYC-WTC_000037113

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