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GCMS analysis results for sample AD26320, Dec 2001

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AD26320 conducted on December 4, 2001.

NYC-WTC_000037104–000037115

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\26320.D Vial: 25 Acq On 16 Dec 2001 1:54 am Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Acetic acid, octadecyl ester Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.77 0.57 ug/1 134558 Chrysene-dl2 33.00

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic aci , octadecyl ester 312 C20H40O2 000822-23-1 49 2 1-Eicosand 298 C20H42O 000629-96-9 46 3 1-Octadecanol 270 C18H380 000112-92-5 38 4 Nonadecanol 284 C19H40O 052783-43-4 35 'Abundance Scan 2912 (31 774 min): 26320.D (-) m/z 43.05 100.00% 43 A

5000- 57 9 69 83 97 111 —Pr Yr I — — i i i r i i

125 139 — -- - r . - 31.40 31.60 31.80 32.00 32.20

miz-> --1 20 40 — I_- m/z 83.00 50.66% 120 140 160 180 200 220 240 Abundance #73048: Acetic acid, octadecyl ester 43

4—

_0 5000 ......... 83 97 31.40 31.60 31.80 32.00 32.20 61 111 m/z 57.00 47.08% i ' ' ' ' i ■ ■ I ■ 1 I lL , 4 17 139 , , 224 , 252 , m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #72723: 1-Eicosanol 43 55 I A 4-A4Aa t —PA I 83 31.40 31.60 31.80 32.00 32.201 97 5000 i m/z 60.9.5 45.85% 71 111

11 ■ i ■ ■ ' ■ i ■ 1 ■ ' i 21.............. ..... 252 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #72026: 1-Octadecanol — TT 114 r j —I— f 40 31.40 31.60 31.80 32.00 32.20 55 m/z 55.00 42.66% 5000- 83 71 27 97

। ■ ■ • ■ । • I.T I I 111 125 ' ' I 1 ■■ 1 । । 224 j . rrr-p-n-n-rm p-rTCIO—Lmn 252 MN 'I' •j—i—'-i—i-1 । T 1 ' i ’ rnlz-> 20 40 60 80 100 '20 140 160 180 200 220 240 31.40 31.60 31.80 32.00 32.20

26320.D GCMS1126.M Fri Dec 28 13:05:57 2001 Page 4

NYC-WTC_000037114

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NYC-WTC_000037114Source: NYC Law Department, mirrored locally

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