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GC/MS calibration data sheet for October 5, 2001

Machine-extracted title · confidence 90%

Laboratory data sheet listing extraction dates and calibration results for deuterated standards.

NYC-WTC_000087980–000087999

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000087990
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NYC 9/11 Public Portal Document

Library 'Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT04 01\LB.D Vial: 9 Acq On 4 Oct 2001 11:22 pm Operator: 209 GALOS Sample 9/24 Inst : GC/MS 209 Mise - Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 5 Acetic acid, octadecyl ester Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

29.77 0.43 ug/1 74341 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

(1/Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 91 2 1-Octadecanol ■ 270 C18H38O 000112-92-5 76 3 17-Pentatriacontene 491 C35H70 006971-40-0 49 4 11-Tricosene 322 C23H46 052078-56-5 43. ^undance Scan 2694 (29.775 min): LB.D (-) m/ Z 43 .'05 100700% iI 43 i 83 5000 111

j.Q.i?,____ __ _________ 29.40 29.60 29.80 30.00 30.20 m/ z 83.05 55.23% •n/z~> 50 100 150 200 250 300 350 400 450 Abundance #73048; Acetic acid, octadecyl ester 4)3

5000 83 29.40 29.60 29.80 30.00 30.20 111 m/z .60.95 46.81% (I ii I 1 1139 224 252 ....................................................... m/z~> 50 100 150 200 250 300 350 400 450 Abundance #72029: 1-Octadecanol 40 . 1 83 5 „ A ' 'I ' ' ' ' I 29.40 29.60 29.80 30.00 30.20 SEE m/z 69.10 46.61% 111

! ,224 252 .................... Ti/2->50 100 150 200 250 300 350 400 450 Abundance #58705:17-Pentatriacontene 40 29.40 29.60 29.80 30.00 30.20 m/z .55.00 46.53% 5000 83

I 111

m/z-> 100 150 200 250 300 350 400 450 29.40 29.60 29.80 30.00 30.20

LB.D NP091101.M Tue Oct 09 12:51:06 2001 Page 5

NYC-WTC_000087990

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NYC-WTC_000087990Source: NYC Law Department, mirrored locally

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