GC/MS analysis results for sample AD22654, Oct 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 11 Acetic ‘acid, octadecyl ester Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 31.87 0.42 ug/1 64407 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual C^Acetic acid, octadecyl ester 312 C20H40O2! 000822-23-1 83 2 17-Pentatriacontene 491 C35H70 006971-40-0 52 3 Cyclotetradecane 196 C14H28 000295-17-0 50 4 1-Docosene 308 C22H44 001599-67-3 49 Abundance Scan 2922 (31.868 min): 22654,0 (-) m/z 43705 TOOTO^ 43 83

5000 111 ’I I ' ' ' ' I ‘ ‘

Tl/Z-> li ■’i 50 i|, kr,............ 100 150 200 250 300 350 400 450 31.60 31.80 32.00 32.20 m/z 83.00 69.82% Abundance #73048: Acetic acid, octadecyl ester 43

5000 83 JUU 31.60 31.80 32.00 32.20 m/z 60795 63.56% I HP'' } 11?9 224 252 n/z-> 50 100 150 200 250 300 350 400 450 Abundance #58705:17-Pentatriacontene 43

31.60 31.80 32.00 32.20 5000 83 m/z 55?^ 62.83%

I 111 I t H i 1 462 490 ■n/z-> ^bundance 50 55 100 150 200 250 300 #69524: Cyclotetradecane 350 400 450 JUL I ' ' ' ' I ' ' 31.60 31.80 32.00 32.20 m/z SYTOO 60.56% 83 5000

27 111 1 168 196 7 V 'n/z-> 50 100 150 200 250 300 350 400 450 31.60 31.80 32.00 32.20

22654.D NP091101.M Fri Oct 12 09:09:26 2001 Page 11

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