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GC/MS analysis results for sample AD22654, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File : 'C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Eicosane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 32.73 5.35 ug/1 830005 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 9K 2 Octadecane 254 C18H38 000593-45-3 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Nbnadecane 268 C19H40 000629-92-5 91/ Abundance Scan 3016 (32.731 min): 22654.D (-) m/z 57.00 100.00% 5/

5000 85

Tlfe-> Abundance lu 40 60 169 ' '' ' ' I 197 225 253 281 352 I ' '' ' I " ' 'I ' ' '' I ' '’' I ' ' ' 'I ' ' '' I ' '' ' I '' ' 'I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #39862: Eicosane -L 32.40 32.60 32.80 33.00 m/z 71.00 A 72.09%

57

5000 85 , l\... 32.40 32.60 32.80 33.00 m/z 43.05 66.46% I, I «l ■'P , 141 196 240 282 I. I I I I T I Ii|I Ir11.I 11fI. I' 'I‘ I '' ' ' I ' ''' I ' I' ‘ 1 I >‘ • I " ' 'I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 57 TT-y—1-1 pr/1 T'—i

32.40 32.60 32.80 33.00 85 5000 m/z 85.00 49.90%

« I IIS 141 224 -n-yn-n-p- '' I " '' I'' " I' " ' I " '' i'' " I " n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201; Heneicosane y V n T' '7 57 32.40 32.60 32.80 33.00 m/z 4170^ 25.92% 5000 85 J I 113 .... J/,..'.......... ???■,, .^..... m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

22654.D NP091101.M Fri Oct 12 09:09:28 2001 Page 12

NYC-WTC_000087483

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NYC-WTC_000087483Source: NYC Law Department, mirrored locally

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