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GC/MS analysis results for sample AD22654, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087484
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NYC 9/11 Public Portal Document

Library Search Compound Report ‘ Data File : C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Heneicosane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.69 6.39 ug/1 990449 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 91' 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91 3 Heptadecane 240 C17H36 000629-78-7 9L 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 3120 (33.686 min): 22654.D (-) m/z 577 CTO 100.00% 7

85

4 5000

Tl/z-> Abundance 40 ib- . 'k li .4 . .. . .225 267 295 TfTSTdYrTTTpVTTfTTTVpdSTYrT ’rT'P’r-rTp-TTTqT-rTTpTTTJTTTTpTTTY'T-TTpTTTJTT-r 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 #42201: Heneicosane 366 m/z 33.40 33.60 33.80 34.00 71.00 I 72.35%

5|7

85 5000 ' ' I 33.40 33.60 33.80 34.00 m/z 43.05 66.62% I 113 , 268 296 A I’ •" I " ••I " Hp. III I'''' I ''I ' Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #50999: Eicosane, 7-hexyl- 7 1 T' ' ' 33.40 33.60 33.80 34.00 5000 85 m/z 85.05 50.01% *

Xu ^®2i97 281 310

4 pTnnq-TTTTp-TTTpn-rTp-rTnTTTT-r^^ " ' F" " I'' *' I * " ' I “ " I' ’' nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #32063: Heptadecane 7 33.40 33.60 33.80 34.00 m/z 41705 25.16% 85 5000

196 240 I ''' ' I''' ‘ I'''' I'''' I I ' ' '' I'"'' I'''' 1'' ‘' I ■nfe-> 6080100120140 160 180 200 220 240 260 280300 320 340 360 33.40 33.60 33.80 34.00

22654.D NP091101.M Fri Oct 12 09:09:30 2001 Page 13

NYC-WTC_000087484

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NYC-WTC_000087484Source: NYC Law Department, mirrored locally

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