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GC/MS analysis results for sample AD22654, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087485
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NYC 9/11 Public Portal Document

Library Search Compound Report

' Data File : C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 2'09 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Eicosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.60 4.82 ug/1 747788 Chrysene-dl2 33.13 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 9L 2 Heneicosane 296 C21H44 000629-94-7 91\ 3 Octadecane 254 C18H38 000593-45-3 91 / 4 Heptadecane ____________________ 240 C17H36 000629-78-7 9K Abundance Scan 3220 (34.604 min): 22654.D (-) m/z 57.00 100.00% 57 J 552 85

4 V JUXu I ' ' ' ' I 34.20 34.40 34.60 34.80 35.00 197 221 239256 295 323 380 mTz 71.00 71.55% j5TT-lYrrrrpTT-rpTTTyrTTTyrTTTpTTTyrTTTpT-rTyr^^ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 ^bundance #39862: Eicosane 57

5000 85 I ' ' ' ' I ‘ ' I ' ' ’ ‘ I ‘ ' 34.20 34.40 34.60 34.80 35.00 m7z 43.00 67.04% 196 240 282 I T 7TTTTpTTTyTTTTyrTTTpT-TT7TTTTpT-rTp-rTTpTTTY^ n/z-> 40 60 80 100 120,140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #42201: Heneicosane 5|7 ■ J[ 85 34.20 34.40 34.60 34.80 35.00 5000 m/z 85.00 49.66%

268 296 ...... .. '' I'''' I'''' I'''' I'' '' I " '' I " Tlfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #71561; Octadecane 57 34.20 34.40 34.60 34.80 35.00 m/z 41.05 24.26% 85 5000

7lfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 1 '”1 ' r

34.20 34.40 34.60 34.80 35.00

22654.D NP091101.M Fri Oct 12 09:09:33 2001 Page 14

NYC-WTC_000087485

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NYC-WTC_000087485Source: NYC Law Department, mirrored locally

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