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GC/MS analysis results for sample AD23321, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23321 conducted on October 15, 2001.

NYC-WTC_000088237–000088262

Folder label: “GC/MS Scan 9/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23321.D Vial: 14 Acq On : 12 Oct 2001 2:50 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Octadecane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.61 2.31 ug/1 290428 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Octadecane 254 C18H38 000593-45-3 91’ 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91 3 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 4 Eicosane 282 C20H42 000112-95-8 91 Abundance Scan 3221 (34.613 min): 23321 .D (-) m/z 57.00 100.00% 57 43 71 5000

I 85

99 ,,... n.... 34.20 34.40 34.60 34.80 35.00 I, ^,1 'Ji, 4,, /J I, .. .I,, "mTz 71705 66.60% 'nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71560: Octadecane 43 5 7

71 5000 85 34.y 34.40 34.60 34.80 35.00 99 "m/z 43705 64.15% J 169183197 I ' I'' I ' ' ' ' I ' ' ' ' I ' I ' ' '' I I' ' ' ' I ' ' ' ' I ' * ' ' I TT/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #50999: Eicosane, 7-hexyl- 43 57 X I * I 71 34.20 34.40 34.60 34.80 35.00 5000 85 m/z 85.05 48.09%

281 310 ' ‘ I' I ' ’IT'' 'I « I » • I « I • • I • t I > j ' I''' I' ' r'''' I " '' I ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #51002: Heneicosane, ll-(l-ethylpropyl)- 4(3 57 34,20 34.40 34.60 34.80 35.00 m/z 41700 23.44% 71

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ifl 99 I 1 II 183197211225 ,, 295 333 ' ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340' 34.20 34.40 34.60 34.80 35.00

23321.D NP091101.M Mon Oct 15 10:22:39 2001 Page 12

NYC-WTC_000088256

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