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GC/MS analysis results for sample AD22979, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22979 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087773–000087793

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0301\22979.D Vial: 5 Acq On 3 Oct 2001 4:33 pm Operator: 209 GALOS Sample gc/ms unknown - Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Octadecane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.71 1.26 ug/1 194948 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91 2 Heneicosane 296 C21H44 000629-94-7 91X 3 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91/ 4 Tetracosane 338 C24H50 ____ 000646-31-1 90 lAbundance Scan 3123 (33.714 min): 22979.D (-) m/z 57.00 100.00% 57 43 71 I 85 5000

JLU 99 ■i. 4 I I I I I i p I |■'l I I I I I'l I ^?7.21.1 227240I 281 A 33.40 33.60 33.80 34.00 I II I T] IT f (' I r I I I I I I I I I I I '' I''' ‘ I'' m/z 71.00 A 68.08% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71561; Octadecane 7

5000 43 71 85 r a 33.40 33.60 33.80 34.00 m/z 43.0.5 63.84% 224 254 I ' ' ' ' I ' ' ' ‘ I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 <\bundance #42201: Heneicosane 57 71 I '-I • 85 33.40 33.60 33.80 34.00 5000 m/z 85.05 53.08% i ; 99 268 296 l-VTT-rjTTTr-ry-r-rn-ipT-rT-ry-rTT-i^^ ' ' ' p ' ’ ‘ p < ' ' p ' p ' ‘ ( nn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #50999; Eicosane, 7-hexyi- 43 57 33.40 33.60 33.80 34.00

71 m/z 41.05 24.44% 5000 85

1 T I ' 169182 197 ’ I * ' ' ' I * 281 310 -p-TT-r -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 33.40 33.60 33.80 34.00

22979.D NP091101.M Tue Oct 09 09:54:41 2001 Page 8

NYC-WTC_000087787

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