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GC/MS analysis results for sample AD22579, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22579 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087180–000087201

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087196
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22579.D Vial: 7 Acq On : 28 Sep 2001 6:18 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Octadecane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 34.64 0.67 ug/1 111210 Chrysene-dl2 33.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 96 2 Tetracosane 338 C24H50 000646-31-1 90 3 Heneicosane 296 C21H44 000629-94-7 90 4 Docosane ____________________ 310 C22H46 000629-97-0 87 Abundance Scan 3225 (34.644 min); 22579. D (-) m/z 57700 100.00% 57

43 71 85 5000 J T" T 256 34.40 34.60 34.80 35.00 m/z: 71.00 67.88% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #71560: Octadecane

5000 43 57

71 85

m/z n 34.40 34.60 34.80 35.00 43 705 64.68% 99 I I J 169183197 2^ I ' ‘ I 1' ' ' ' I ' ' ' ' I -nlz-> 40 60 80 100 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543; Tetracosane 43 57 71 34.40 34.60 34.80 35.00 5000 85 m/z: 85.00 50.41%

99 t I ll 155169183197 294 338 pnVrjJFrTTY7'TVTyT¥TTyT-TTAjT-¥TnrjVTTrpnT-rp-rTT-pTTTy^ I' " 'I ‘ Tife-> 'Xbundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #42201: Heneicosane T JV I ' ' 5(7 34.40 34.60 34.80 35.00 71 "mTz 41705 25.90% 85 5000

99

4XjiTrTrpnrTTYTVTTq^TTTr+p-rTTpT-rTp-m-pT-rTp-rTTpTT-rp-rr+yTT-^^ nife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34,40 34,60 34.80 35.00

22579.D NP091101.M Tue Oct 02 11:50:23 2001 Page 10

NYC-WTC_000087196

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NYC-WTC_000087196Source: NYC Law Department, mirrored locally

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