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GC/MS analysis report for sample AD22494, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22494 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086852–000086871

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086859
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2501\22494.D Vial: 5 Acq On : 25 Sep 2001 6:21 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Octadecane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

34.64 2.80 ug/1 318038 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91 2 Tetracosane 338 C24H50 000646-31-1 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Tetratetracontane 619 C44H90 007098-22-8 91 Abundance Scan 3225 (34.644 min): 22494.D (-) m/z 57.00 100.00% 57 71 43 85 553 ■i-A-rT= , .j. j'l ,'l;, ,4,, I.... I'" 'I■ _3440_3460_^£80_35W_ m/z 71.00 73721% ttZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 57 43 71 85 5000 T 34.40 34.60 34.80 35.00 m/z 43705 67:77% I, I TT^27141155 224 254 Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71 34.40 34.60 34.80 35.00 5600- 85 m/z 85.00 52.41%

l| /;^127 155169183197 I I I ' '' ' I 1 ■ r I ■ I ■ • • I ■ • ■ ■ 11 • H 1. 1111 "i''"' I •' '' I'' 294 338 nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 34.40 34.60 34.80 35.00 71 m/z 41700 21.14% 85 5000

99

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.40 34.60 34.80 35.00

22494.D NP091101.M Wed Sep 26 15:26:52 2001 Page 6 NYC-WTC_000086859

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NYC-WTC_000086859Source: NYC Law Department, mirrored locally

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