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GC/MS analysis report for sample AD22494, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22494 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086852–000086871

Folder label: “508 Scan 9/15/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22494.D vial: 5 Acq On : 25 Sep 2001 6:21 pm Operator: 209 GALOS Sample : GC/MS unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Pentacosane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.72 3.70 ug/1 421131 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentacosane 352 C25H52 000629-99-2 91 / 2 Heneicosane 296 C21H44 000629-94-7 91 ( 3 Eicosane 282 C20H42 000112-95-8 91 \ 4 Eicosane, 7-hexyl-_____________________ 366 C26H54 055333-99-8 91 ^^undance Scan 3124 (33.717 min): 22494.D (-) m/z SYTOO 100.00% 57 43 71 85 5000 ... I[.... in 33.40 33.60 33.80 34.00

n/z-> 40 UL ,ll, iJ J 155 169183 197 211 225239253267281 m/z 71.05 I "' ' I I ' '' ' I ''' ' I 11 I I I I I I' 11 I

60 80 100 120 140 160 180 200 220 240 260 280 300 ' I I' 11 1 ■>' I I I I ' I ■ ' ' I' ' ' ' I ' ' I I I ' 71.59% Abundance #73718: Pentacosane 43 57

71 5000 85 33.40 33.60 33.80 34.00 m/z 43.05 68.25% I •n/z-> 40 60 I 80 II T. 100. 120 140 160 180 200 220 240 260 280 300 1 ' ' ' ' I

Abundance #42201: Heneicosane 5)7 71 85 iX 33.40 33.60 33.80 34.00 5000 m/z 85.05 49.47%

99 ......................................... 268 J96 ‘ ' i ' ' iiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #39862: Eicosane 43 5)7 ^.40 33.60 33.80 34.00 m/z 55.00 24.50%

5000 71 85 ft ' ' I ‘ 1 T 196 240 282 ' I ' ' _J L I'''' I niZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 33.40 33.60 33.80 34.00

22494.D NP091101.M Wed Sep 26 15:26:50 2001 Page 5 NYC-WTC_000086858

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NYC-WTC_000086858Source: NYC Law Department, mirrored locally

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