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GC/MS analysis results for sample AD23497, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.

NYC-WTC_000088753–000088773

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088767
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1601\23497.D Vial: 5 Acq On : 16 Oct 2001 6:08 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Pentacosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 32.73 0.60 ug/1 63004 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qua!

ML Pentacosane 352 C25H52 000629-99-2 91 2 Tetracosane 338 C24H50 000646-31-1 87 3 Heneicosane 296 C21H44 000629-94-7 87 4 Nonacosane ____________________ 408 C29H60 000630-03-5 86 Abundance Scan 3017 (32.734 min): 23497. D (-) m/z SYTOO 100.00% 5)7

71 43 85 5000

nZz-> Abundance 40 w 60 1 iJ ^]'^127141155169 207 I'T'i . q 117. 11'\ 111111 -111 I i-i 11 ■ ■ ■ I ■ ■ ■ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73718: Pentacosane I ' ' ' ’ 1 32.40 32.60 32.80 33.00 m/z 71.00 ■’ I ' ' ' ' I

68.92%

z 3 5|7

71 5000 85 32.40 32.60 32.80 33.00 m/z 43.05 62.25% I T ^1^''?^''^'*''55169183197211225 I'''' I I'' " I'''' I'"' i Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ‘Abundance #73543: Tetracosane 43-517----- 71 32.40 32.60 32.80 33.00 553 85 m/z85.05 51.40%

l|Jp127 155169183197 „294 338 pr-r T ' I'''' I '' I'''' r n/z-> 40 60 80 100 120 140 160 180 200 220 240 '260 280 300 320 340 Abundance 57 #42201: Heneicosane .-JU 32.40 32.60 32.80 33.00 71 m/z'-^ 4-1^05- 28.02% 85 5000

99

■nfe-> 40 JU 60 268 ' I ''"' I ' ' ' ’ I' ‘ 296 ' I -p-r-rTp-T-rry 80 100 120 140 160 180 200 220 240 260 280 300 320 340 yTnT|-n-rlyi A 32.40 32.60 32.80 33.00

23497.D NP091101.M Thu Oct 18 10:07:40 2001 Page 8

NYC-WTC_000088767

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