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GC/MS analysis results for sample AD23497, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.

NYC-WTC_000088753–000088773

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088768
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23497.D Vial: 5 Acq On : 16 Oct 2001 6:08 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params-. LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ************************************************** * * ***************** Peak Number 9 Hexadecane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 33.69 0.73 ug/1 76230 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolFortn CAS# Qual

Hexadecane 226 C16H34 000544-76-3 95 Heptadecane 240 C17H36 000629-78-7 94 3 Pentacosane 352 C25H52 000629-99-2 87 4 Nonacosane ____________________ 408 C29H60 000630-03-5 87 Abundance Scan 3121 (33.689 min): 23497.D (-) m/z 57.00 100.00% 57 43 71

85 5000

33.40 33.60 33.80 34.00

TiZz-> 40 Mr 60 I 80 ' I''' ' I ‘‘ I'''' 11 ■' ■ 1, ■ • 11. ■ 111 ■ 11111", 1. 11, 100 120 140 160 180 200 220 240 m/z 71.00 A 72.79% Abundance #70788: Hexadecane 5|7 43 71 5000 k 85 33.40 33.60 33.80 34.00 m/z 43.05 72.43% 99 .113 127 141 155 169 183 226 TlZz-> 40 60 80 100 120 140 160 180 200 220 240. Abundance #71193: Heptadecane 5|7-

71 ■ 33,40 33.60 33.80 34.00 5000 m/z 85.05 52.99% 85

99 .4 .. .. ni/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #73718: Pentacosane 4)3 5,7 ----- -33.40- 33.60 -33.80 34.00 'm/z 41-. 05 - 26.18% 71 5000- 85 , ,A A I I I I .'.^1 . .V 99 hl 141 155 169 183 197 211 225 T n/z-> 40 60 80 100 120 140 160 180 200 220 240 • 33,40 33.60 33,80 34.00

23497.D NP091101.M Thu Oct 18 10:07:42 2001 Page 9

NYC-WTC_000088768

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NYC-WTC_000088768Source: NYC Law Department, mirrored locally

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