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GC/MS analysis results for sample AD23650, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23650 conducted on October 19, 2001.

NYC-WTC_000089000–000089024

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound-Report Data File : C:\HPCHEM\1\DATA\OCT1601\23650.D Vial: 15 Acq On : 17 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Hexadecane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 33.69 1.55 ug/1 188790 Chrysene-dl2 33.13

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

Hexadecane 226 C16H34 000544-76-3 96 Pentacosane 352 C25H52 000629-99-2 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Octadecane 254 C18H38 000593-45-3 91 Abundance Scan 3120 (33.687 min): 23650.D (-) m/z 57.00 100.00% 57 43 71

5000 85

k .J 151 155 169 183 197210 226 240 , i' I . . I I , . I . I . , . . I . . . , I . I', , II . I ■. . I I I I I , . I . I , I . . I . , . . I I K 33.40 33,60 33.80 34.00 m/z 43.05 71.56% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 . 280 300 Abundance #70788: Hexadecane 57 43 71 5000 85 33.40 33.60 33.80 34.00 m/z 71.10 70.95% 99 113 127141 155169 183 ..LI 226 nn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance —#73718;-Pentacosane------------ 43 5,7

71 Ik 33.40 33.60 33.80 34.00 5000 85 m/z 85.05 49.84%

mfe-> uLUU 100/L 120 140 160 180 200 220???..................... 40 60 80 240 260 280 300 Abundance #42201: Heneicosane_ _ 57 ■33.40 ^ 33.60 - 33,80 • 34.00' - 71 m/z 41.05 24.65% 85 5000

99

Tl/z-> 40 uu 60 80 ‘I ’ ' I ' 1 ' ' ' ' I ' ' ' ' I 100 120 140 160 180 200 220 240 260 280 300 33.40 33.60 33.80 34.00

23650.D NP091101.M Thu Oct 18 10:40:29 2001 Page 12

NYC-WTC_000089018

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NYC-WTC_000089018Source: NYC Law Department, mirrored locally

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